Comments (3)
7 March '22
- dissolved 1.9546 g (9.76 mmol) cyclam in 100 mL water
- chilled in ice bath
- added 1.6 mL (21.2 mmol) formaldehyde at 2.02 pm
- immediately formed cloudy white precipitate
- vacuum filtered at 3.15 pm and left to dry
from usyd_phd_eln.
8 March 2022
- vial (empty) = 15.9339
- vial (full) = 17.2961
- mass = 1.3622 g
from usyd_phd_eln.
23.06.22
NMR
Indicates product was successfully made.
from usyd_phd_eln.
Related Issues (20)
- KBS44-2 - Nosyl deprotection of KBS49 HOT 12
- KBS50-2 - Nosyl protection of bis(3-aminopropyl)amine HOT 9
- KBS53-1 - Nosyl deprotection of KBS48 HOT 13
- KBS52-1 - Nosyl deprotection of KBS51 HOT 7
- KBS51-1 - Mitsunobu reaction with KBS28 and KBS50 HOT 10
- KBS53-2 - Nosyl deprotection of KBS48 HOT 11
- KBS48 (pooled) - purification HOT 3
- KBS52-2 - Nosyl deprotection of KBS51 HOT 2
- KBS51-2 - Mitsunobu reaction with KBS28 and KBS50 HOT 5
- KBS22-2 - Linear click coupling of bis-propargyl diaminohexane and azidoadamantane HOT 6
- Carlota's compounds - for purification HOT 2
- KBS22-3 - Linear click coupling of bis-propargyl diaminohexane and azidoadamantane HOT 8
- KBS52-3 - Nosyl deprotection of KBS51 HOT 16
- 2024_BG_A_1 - Formation of benzoyl thioureas HOT 2
- 2024_BG_B_1 - Hydrolysis of benzoyl thioureas HOT 2
- SAR - for future aminothiazoles
- 2024_BG_C - characterisation of final compounds HOT 6
- 2023_BG_12C
- HPLC results for various samples (BG_8J, 2022_BG_8B, 2022_BG_8C, CRM3) HOT 4
- KBS13-1 HOT 1
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